Buy ASTM D TEST METHODS FOR CARBON BLACK – DISPERSION IN RUBBER from SAI Global. However, unvulcanized compounds should be compressed in a mold for 5 minutes at °C to remove the air holes before testing. ASTM D , Method B , is a. ASTM D Standard Test Methods for Carbon Black-Dispersion in Rubber.

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If a die is not used, the specimen length and width should be recorded using a measuring magni? The life of a knife depends very much on the number of sections that are cut particularly in paring down the sample block and in the nature of the sample itself. This applies only to vulcanized specimens.

Such samples are quite tedious to measure. The dispersion level of the carbon black is compared against a series of?

Standard – Standard Test Methods for Carbon Black-Dispersion in Rubber ASTM D –

Four test methods are described as follows:. Refreeze during the sectioning operation whenever necessary.

Differences are best resolved at somewhat higher magni? Adtm strains are encountered in the latter procedure, and irregularities may occur on the side faces on which the knife edge will be formed.


Originally published as D — 67 T. Careful manipulation of the solvent wet brush will unroll and spread the section out?

Standard Test Methods for Carbon Black-Dispersion in Rubber

Three test methods are described as follows: This adjustment must be coordinated with a correction in the opposite direction for the overall height of the stylus probe. The top of the screw d26633 shall be cross-hatched with? The precison parameters should not be used for acceptance or rejection testing of any group of materials without documentation that they are applicable to those materials and the speci? Test Method C—Microroughness Measurement. This setting will remain constant for subsequent specimens which can simply be mounted in place by gently lifting the stylus with a?

Use a cutting die, if available. Next, reimmerse the specimen mount in liquid nitrogen for the required amount of time. ASTM D e1. After a few seconds the mucilage will freeze and turn white.

Take care again that the score mark does not go all the way out to the edges of the glass. The front edges of the plier jaws should be perpendicular to the score line.

Rubbers that contain relatively high amounts of inorganic pigments are particularly prone to cause knife chipping and may require a fresh knife for each different specimen. Then, the volume percentage of black can be calculated from the following simpli?


If at all possible, examine compounds of this type also by the agglomerate count method, at least until sufficient experience is gained to recognize dispersion differences with the Visual Inspection Method. This represents an x2663 of the?

Standard Test Methods for Carbon Black—Dispersion in Rubber

Then assign the most closely matched numerical rating to each compound being rated. Firm pressure will readily cause fracture. These constants are speci?

Stay within 1 to 2 mm of each side. Coarse, expansion-type threads should be used to prevent splitting of the TFE-? F 5 the number of roughness peaks per cm, and H 5 the number average peak height,? In instances of high agglomerate frequency, the surface of stocks of this type may show a general roughness or? The product of these dimensions is the area after swelling. Steel knives may also be employed, according to the preference of the operator.